NICOTINE BASED PRODUCTS (NICOTINE SULPHATE 40%, NICOTINE ALKALOID 95%, NICOTINE USP/EP, NICOTINE POLACRILEX, NICOTINE BITARTRATE DIHYDRATE)

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From harvesting of tobacco to manufacture of products, large quantities of waste materials comprising rejected leaves broken bits of lamina nidribs, stalks and stems accumulate such materials however can be utilized with considerable benefit. Nicotine and tobacco seeds are by far the most important by products derived from tobacco waste.

In addition many other chemicals like nicotine acid, nicotine sulphate, rutin, pectic and certain organic acids can be produced from these wastes.

The average nicotine content in Indian tobacco waste is 1-3% waste containing even less than 2 percent nicotine can be utilized. A simple and economic process by which about 95% of the nicotine present in tobacco waste can be recovered as nicotine sulphate has been developed by National Chemical Laboratory, Poona, and is being commercially exploited by Tobacco By Products Ltd., Guntur Urvakunj Tobacco by Products, Dharmaj (Gujarat) is also one of the nicotine sulphate manufacturing units.

Nicotine sulphate is extensively used in the control of insect pest of agricultural importance. It is being manufactured from waste tobacco and from the liquors obtained from factories making chewing and smoking tobacco. The waste tobacco is macerated with water and lime and then steam distilled. The distillate is neutralized with sulphuric acid and concentrated.

TOBACCO INDUSTRY AND EXPORT

Tobacco in India was introduced by Portuguese in the 17th century, is appreciated worldwide for its rich, full-bodied flavour and smoothness. It is now an increasingly well-known and respected commodity in global tobacco markets and has found its way into cigarettes manufactured in several countries. India has an impressive and progressive profile in the global tobacco industry, and it is an important commercial crop grown here. India is the second-largest tobacco producer and exporter in the world.

Tobacco Exports from India and Key Markets

• The tobacco export in the month of August 2021 was US$ 72.28 million and the total export during April 2021 to August 2021 was 386.08 million.

• The tobacco export in the month of March 2021 was US$ 85.52 million and the total export during FY21 was US$ 875.09 million.

• In FY21, export of unmanufactured tobacco stood at US$ 517.54 million.

• The total export of flue-cured Virginia (FCV) tobacco in July 2021, was US$ 18.7 million, while for a period from April 2021 to July 2021, it was US$ 139.6 million.

• India export unmanufactured tobacco primarily to Belgium, Korea, Nigeria, Egypt and Nepal. Western Europe is a key market for Indian tobacco export.

Foreign Direct Investment in Tobacco Industry in India

In August 2020, the parliamentary panel proposed permitting regulated foreign direct investment in India’s tobacco production and cigarette manufacturing to stimulate agricultural exports.

The panel proposed establishment of tobacco farms dedicated to exports only to improve outward shipments and to provide benefits to farmers. It also suggested to provide export incentives for tobacco and tobacco products.

Tobacco Board

The Tobacco Board of India is a facilitator for tobacco growers, traders and exporters. By creating synergies between these stakeholders, the Board fosters a vibrant enterprise, with a deep social conscience and strong national commitment. The Board estimates demand and regulates the production of FCV tobacco to match demand to ensure a fair price for the produce. It assists tobacco farmers in securing crop loans, quality seeds, fertilisers and other critical inputs, and also counsel’s farmers on GAP to produce quality tobaccos to meet the evolving international demand. In addition, the Board conducts auction for the sale of tobacco in a competitive and transparent environment. On the export front, the Board strives to improve the existing markets and develop new markets for Indian tobacco and tobacco products by undertaking brand building exercises and participation in international tobacco exhibitions.

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Description

INTRODUCTION
TOBACCO INDUSTRY AND EXPORT
TOBACCO EXPORTS FROM INDIA AND KEY MARKETS
FOREIGN DIRECT INVESTMENT IN TOBACCO INDUSTRY IN INDIA
TOBACCO BOARD
TOBACCO IN INDIAN ECONOMY
POSITIVE FEATURES OF INDIAN TOBACCO
IMPACT OF TOBACCO RESEARCH
USES AND APPLICATION OF NICOTINE BITARTRATE DIHYDRATE
USES AND APPLICATIONS OF NICOTINE SULPHATE
PROPERTIES OF NICOTINE SULPHATEAZARD AND SHIPPING REGULATION:
APPLICATION OF NICOTINE POLACRILEX
ADVANTAGE OF NICOTINE POLACRILEX
NICOTINE POLACRILEX/RESINATE USP/EP 20%
NICOTINE POLACRILEX/RESINATE USP/EP 15%
B.I.S. SPECIFICATION
1. SCOPE
2. REQUIREMENTS
3. PACKING AND MARKING
4. SAMPLING
5. TESTS
DETERMINATION OF NICOTINE CONTENT
A – 1 METHOD
A – 2 REAGENTS
SEDIMENTATION TEST
B – 1 PROCEDURE
B – 2 REPORT
NICOTINE SULPHATE 40%
CHEMICAL COMPOSITION:
MODE OF ACTION:
USES:
CHEMICAL FORMULA:
ADVANTAGES:
NICOTINE SULPHATE 40%
USES AND APPLICATION OF NICOTINE ALKALOID 95%
NICOTINE ALKALOID 95%
SPECIFICATIONS
OTHER INFORMATION
PROPERTIES OF NICOTINE POLACRILEX 20%
PRODUCT SPECIFICATION:
COMPOSITION:
MARKET OVERVIEW OF NICOTINE SULPHATE
MARKET OVERVIEW OF NICOTINE AND NICOTINE PRODUCTS IN INDIA
PRODUCTS FROM TOBACCO AND TOBACCO WASTES:
NICOTINE/NICOTINE DERIVATIVES FROM TOBACCO:
NICOTINE AND ITS COMMERCIALLY IMPORTANT DERIVATIVES:
WORLD PESTICIDE MARKET AND PROSPECTS FOR NICOTINE SULPHATE
STATUS OF TOBACCO WASTE BASED INDUSTRIES IN INDIA
OVERVIEW OF TECHNOLOGIES FOR NICOTINE BASED PRODUCTS
NEED FOR DEVELOPMENT OF ALTERNATE USE FOR TOBACCO:
[COMMERCIALLY IMPORTANT APPLICATIONS]:
A LOOK AT THE ORGANS OF THE BODY HARMED BY TOBACCO SMOKE
PHARMACEUTICAL USE OF NICOTINE:
COMMERCIAL ASPECTS OF NICOTINE SULPHATE & NICOTINE DERIVATIVES
CONCLUSIONS AND RECOMMENDATIONS:
SOME OF THE IMPORTANT PATENTED PROCESS INCLUDES:
RECOMMENDATIONS:
MARKET OVERVIEW OF NICOTINE POLACRILEX
LIST OF THE COMPANIES OPERATING IN THE MARKET:
FURTHER REPORT FINDINGS:
MARKET OVERVIEW OF NICOTINE GUMS
PRESENT MANUFACTURERS/SUPPLIERS OF NICOTINE BASED PRODUCTS
CHEMICAL COMPOSITION OF TOBACCO
CHEMISTRY OF NICOTINE
THE DISTILLATION AND CONCENTRATION INSTALLATION WAS
BUILT UP AS FOLLOWS:
(1) THE STEAM DISTILLATION KETTLE.
(2) THE STEAM-HEATED NICOTINE CONCENTRATION CHAMBER.
(3) THE NICOTINE CONCENTRATIOIN FLASKS.
(D) THE DISTILLATION AND CONCENTRATION PROCESS.
(1) THE CONCENTRATION OF THE ACID IN THE FLASKS.
(2) THE TEMPERATURE OF THE CONCENTRATION CHAMBER
(3) THE DLSTILLATION PERIOD.
(4) THE AMMONIUNN SULPHATE FORMED IN ‘THE RECEIVING FLASKS.
(5) THE SEPARATION OF THE AMMONIUM SULPHATE AND NECOTINESULPHATE
VALUE OF BY PRODUCTS
THE EXTRACTED TOBACCO RESIDUE
COMMERCIAL
CHARACTERISTICS & APPLICATION OF NICOTINE:
ZONES OF CULTIVATION OF TOBACCO:
RAW MATERIALS
TOBACCO:
GLOBAL PRODUCTION
TRENDS
MAJOR PRODUCERS
UNITED STATES
CHINA
BRAZIL
INDIA
BENZENE:
HAZARD:
LIME:
HAZARD:
SULFURIC ACID:
HAZARD:
TOBACCO LEAF BY-PRODUCTS (TOBACCO WASTE)
DETAILS OF NICOTINE BASED PRODUCTS MANUFACTURE
DETAILS OF NICOTINE ALKALOID 95% MANUFACTURE
DETAILS OF NICOTINE BASE USP/EP MANUFACTURE
DETAILS OF NICOTINE POLACRILEX/RESINATE USP/EP)
MANUFACTURING PROCESS OF NICOTINE USP/EP
MASS BALANCE PER MONTHSFOR NICOTINE USP/EP
MANUFACTURING PROCESS OF NICOTINE POLACRILEX (USP/EP)
MASS BALANCE PER MONTHSFOR NICOTINE POLACRILEX USP/EP
MANUFACTURING PROCESS OF NICOTINE BITARTRATE DIHYDRATE
CHEMICAL REACTION
MASS BALANCE PER MONTHSFOR NICOTINE BITARTRATE DIHYDRATE
MATERIALS BALANCE SHEET FOR NICOTINE BITARTRATE DIHYDRATE
DETAILS OF NICOTINE BITARTRATE DIHYDRATE MANUFACTURE
MATERIAL BALANCE SHEET FOR NICOTINE DIHYDRATE
OUT/KGS OF PRODUCT (KGS)
MANUFACTURING PROCESS OF NICOTINE 95%
MANUFACTURING PROCESS NICOTINE SULPHATE (40%)
PROCESS DETAILS OF NICOTINE (USP)
PROCESS FLOW DIAGRAM
PROCESS FLOW SHEET FOR NICOTINE SULPHATE FROM TOBACCO WASTE
PROCESS FLOW DIAGRAM FOR NICOTINE
PROCESS FLOW DIAGRAM FOR NICOTINE POLACRLEX
PROCESS FLOW DIAGRAM FOR NICOTINE DITARTRATE DIHYDRATE
HAZARDOUS FACT SHEET FOR NICOTINE SULPHATE
HAZARD SUMMARY
IDENTIFICATION
REASON FOR CITATION
HOW TO DETERMINE IF YOU ARE BEING EXPOSED
WORKPLACE EXPOSURE LIMITS
WAYS OF REDUCING EXPOSURE
HEALTH HAZARD INFORMATION
ACUTE HEALTH EFFECTS
CHRONIC HEALTH EFFECTS
CANCER HAZARD
REPRODUCTIVE HAZARD
OTHER LONG TERM EFFECTS
MEDICAL
MEDICAL TESTING
EKG
CONDITIONS MADE WERSE BY EXPOSURE
WORKPLACE CONTROLS AND PRACTICES
IN EVALUATING THE CONTROLS PRESENT IN YOUR WORKPLACE, CONSIDER
IN ADDITIONS, THE FOLLOWING CONTROL IS RECOMMENDED:
PERSONAL PROTECTIVE EQUIPMENT
CLOTHING
EYE PROTECTION
RESPIRATORY PROTECTION
IMPROPER USE OF RESPIRATORS IS DANGEROUS
IMPLEMENTATION SCHEDULE:
MATERIAL SAFETY DATA SHEET OF NICOTINE SULPHATE 40%
PROCESS DESCRIPTION & MATERIAL BALANCE OF NICOTINE SULPHATE 40%
OVERALL MATERIAL BALANCE
BASIS: 60 MT /MONTH
EXPORTER OF NICOTINE BASED PRODUCTS
CONSULTANT & TECHNOLOGY SUPPLIERS
TESTING METHOD OF NICOTINE AND NICOTINE SULPHATE
EXAMPLE L
STAGE 1 HARVESTING AND DEEP FREEZING
STAGE II MIXING AND PERCOLATION
STAGE III EXTRACTION
STAGE IV SEPARATION
STAGE V FILTRATION AND PURIFICATION
STAGE VI TESTING
STAGE VII PACKING
EXAMPLE 2
STAGE 1 MIXING
STAGE II PERCOLATION
STAGE III EXTRACTION
STAGE IV SEPARATION
STAGE V FILTRATION AND PURIFICATION
STAGE VI PACKING
STAGE VII ALKALIZATION
STAGE VIII PURIFICATION OF NICOTINE ALKALOID
STAGE IX DISTILLATION OF NICOTINE ALKALOID
STAGE X TESTING
STAGE XI PACKING
EXAMPLE 3
STAGE 1 MIXING
STAGE II MIXING AND PERCOLATION
STAGE III EXTRACTION
STAGE IV SEPARATION
STAGE V FILTRATION AND PURIFICATION
STAGE VI PACKING
STAGE VIII PURIFICATION OF NICOTINE ALKALOID
STAGE IX DISTILLATION OF NICOTINE ALKALOID
STAGE X TESTING
STAGE XI PACKING
EXAMPLE 4
STAGE 1 MIXING
STAGE II PERCOLATION
STAGE III EXTRACTION
STAGE IV SEPARATION
STAGE V FILTRATION AND PURIFICATION
STAGE VI PACKING
STAGE VII ALKALIZATION
STAGE VIII PURIFICATION OF NICOTINE ALKALOID
STAGE IX DISTILLATION OF NICOTINE ALKALOID
STAGE X TESTING
STAGE XI PACKING
EXAMPLE 5
STAGE I WASHINGS OF THE INSOLUBLE FRACTION
STAGE II CENTRIFUGATION AND DRYING OF INSOLUBLE FRACTION
STAGE III CENTRIFUGATION AND DRYING OF INSOLUBLE FRACTION
STAGE IV RECONSTITUTION OF THE TOBACCO BY IMPREGNATION
STAGE V TESTING OF THE TOBACCO
STAGE VI PACLDNG
TECHNOLOGY SUPPLIERS FOR NICOTINE BASED PRODUCTS
SUPPLIERS OF RAW MATERIALS
SUPPLIERS OF TOBACCO WASTE
SUPPLIERS OF BENZENE
SUPPLIERS OF LIME POWDER
SUPPLIERS OF PLANT & MACHINERY
SUPPLIERS OF REACTION VESSEL
SUPPLIERS OF INDUSTRIAL FILTERS
SUPPLIERS OF DISTILLATION UNITS
SUPPLIERS OF EVAPORATORS
SUPPLIERS OF TRAY DRYER
SUPPLIERS OF DIGESTER TANKS
SUPPLIERS OF CRYSTALLIZATION TRAY
SUPPLIERS OF CENTRIFUGE MACHINE
SUPPLIERS OF STORAGE TANK
SUPPLIERS OF WATER SOFTENING PLANT
SUPPLIERS OF STEAM BOILERS
SUPPLIERS OF GENERATOR (D.G. SET)
SUPPLIERS OF PACKING MACHINE
SUPPLIERS OF CONVEYOR BELT
SUPPLIERS OF ELEVATORS, ESCALATORS

APPENDIX – A:

01. PLANT ECONOMICS
02. LAND & BUILDING
03. PLANT AND MACHINERY
04. OTHER FIXED ASSESTS
05. FIXED CAPITAL
06. RAW MATERIAL
07. SALARY AND WAGES
08. UTILITIES AND OVERHEADS
09. TOTAL WORKING CAPITAL
10. TOTAL CAPITAL INVESTMENT
11. COST OF PRODUCTION
12. TURN OVER/ANNUM
13. BREAK EVEN POINT
14. RESOURCES FOR FINANCE
15. INSTALMENT PAYABLE IN 5 YEARS
16. DEPRECIATION CHART FOR 5 YEARS
17. PROFIT ANALYSIS FOR 5 YEARS
18. PROJECTED BALANCE SHEET FOR (5 YEARS)

Additional information

Plant Capacity

1.12 MT/Day
Land & Building

(9600 sq.mt.)
Plant & Machinery

US$ 394285
Rate of Return

65%
Break Even Point

29%

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