PHARMA GRADE FERROUS SULPHATE HEPTAHYDRATE

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Ferrous Sulphate ‘Copperas’ Green Copperas, Green Vitriol; FeSO4. 7H2O is obtained as pale green crystals soluble in water. It is produced as a byproduct from waste pickling liquors of galvanizing and tin plates plants or by dissolving scrap iron in warm dilute sulphuric acid. In the bye product process the liquor is treated with scrap iron to reduce the free acid content, neutralized with alkali, filtered and concentrated in evaporators. Alternately, scrap iron and sulphuric acid are added at 180oF, to the liquor to raise the concentration to 430Be. The hot concentrated liquor is introduced into crystallizers and cooled to room temperature. Crystals of heptahydrate separate until the specific gravity falls to 260Be. The crystals are filtered, washed in a centrifuge, broken, screened and dried with warm air at 140oF in rotary drum, dryers. The mother liquor is returned to the neutralizing tank or further concentrated in evaporators. A slight excess of sulphuric acid is usually maintained in the crystals to prevent oxidation; surface oxidation may be counteracted by adding a small quantity of iron to the liquor during the heating and settling operations.

Ferrous Sulphate is also obtained as a bye product in the manufacture of titanium pigment and copper sulphate. For medicinal use, it is prepared by the action of dilute sulphuric acid on iron. Exsiccated Ferrous Sulphate used in therapy is a grayish white powder prepared by drying Ferrous Sulphate crystals at 40oC when a part of the water of crystallization is removed. It is slowly but almost completely soluble in freshly boiled cooled water.

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Description

INTRODUCTION
THE COMMERCIAL METHODS OF ITS DERIVATION ARE:-
PROPERTIES
GRADES OF FERROUS SULPHATE
CONTAINERS AND REGULATIONS
USES AND APPLICATIONS
(I) TECHNICAL GRADE
(II) PURE GRADE
B.I.S. SPECIFICATION
SOLUBILITY:
TABLE-1
TABLE-II
TABLE-III
PACKING & MARKING:-
SPECIFICATION OF FERROUS SULPHATE HEPTAHYDRATE
FERROUS SULPHATE HEPTAHYDRATE AR/ACS MEETS ANALYTICAL
SPECIFICATION OF IP, BP, USP, PH.EUR.
MARKET POSITION OF FERROUS SULPHATE
FERROUS SULFATE MARKET HITS GOLDMINE AS FERROUS SALTS
GAIN POPULARITY TO TREAT ANEMIA
FOCUS ON IMPROVING WATER QUALITY TRIGGERS DEMAND
FOR FERROUS SULFATE
KEY PRODUCT IN FERROUS SULFATE MARKET
HIGH DEMAND FOR FERROUS SULFATE IN VARIOUS INDUSTRIES
ASIA PACIFIC TO BE HIGHLY LUCRATIVE REGION OF FERROUS
SULFATE MARKET
FERROUS SULFATE MARKET: COMPETITION LANDSCAPE
MANUFACTURING PROCESS OF FERROUS SULPHATE
HEPTAHYDRATE (PHARMA GRADE) 26
RAW MATERIALS
CHEMICAL REACTION
PROCESS FLOW DIAGRAM
PROCESS IN DETAILS
REACTION:
FILTERATION:
EVAPORATING:
CENTRIFUGATION:
DRYING:
PROCEDURE:
CALCULATION:
PACKING:
PURIFICATION:
REAGENTS:
METHOD OF FERROUS SULPHATE PRODUCTION
PICKLE LIQUOR REMOVES OXIDE LAYER
THE SULFATE PROCESS
FORMULATIONS/PREPARATIONS
PRODUCTION OF FERROUS SULPHATE HEPTAHYDRATE
FROM FERROUS SULPHATE MONOHYDRATE
POLLUTION CONTROL IN THE MANUFACTURE
OF FERROUS SULPHATE 37
PRINCIPLES OF PLANT LAYOUT
PLANT LOCATION FACTORS
PRIMARY FACTORS
1. RAW-MATERIAL SUPPLY:
2. MARKETS:
3. POWER AND FUEL SUPPLY:
4. WATER SUPPLY:
5. CLIMATE:
6. TRANSPORTATION:
7. WASTE DISPOSAL:
8. LABOR:
9. REGULATORY LAWS:
10. TAXES:
11. SITE CHARACTERISTICS:
12. COMMUNITY FACTORS:
13. VULNERABILITY TO WARTIME ATTACK:
14. FLOOD AND FIRE CONTROL:
EXPLANATION OF TERMS USED IN THE PROJECT REPORT
1. DEPRECIATION:
2. FIXED ASSETS:
3. WORKING CAPITAL:
4. BREAK-EVEN POINT:
5. OTHER FIXED EXPENSES:
6. MARGIN MONEY:
7. TERM LOANS:
8. TOTAL LOAD:
9. LAND AREA/MAN POWER RATIO:
PROJECT IMPLEMENTATION SCHEDULES
INTRODUCTION
PROJECT HANDLING
PROJECT SCHEDULING
PROJECT CONSTRUCTION SCHEDULE
TIME SCHEDULE
SUPPLIERS OF RAW MATERIALS
SUPPLIERS OF PLANT AND MACHINERY

APPENDIX – A:

01. PLANT ECONOMICS
02. LAND & BUILDING
03. PLANT AND MACHINERY
04. OTHER FIXED ASSESTS
05. FIXED CAPITAL
06. RAW MATERIAL
07. SALARY AND WAGES
08. UTILITIES AND OVERHEADS
09. TOTAL WORKING CAPITAL
10. TOTAL CAPITAL INVESTMENT
11. COST OF PRODUCTION
12. TURN OVER/ANNUM
13. BREAK EVEN POINT
14. RESOURCES FOR FINANCE
15. INSTALMENT PAYABLE IN 5 YEARS
16. DEPRECIATION CHART FOR 5 YEARS
17. PROFIT ANALYSIS FOR 5 YEARS
18. PROJECTED BALANCE SHEET FOR (5 YEARS)

Additional information

Plant Capacity

600 Ton/Day
Land & Building

(700 sq.mt.)
Plant & Machinery

US$.14286
Rate of Return

25%
Break Even Point

65%

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